29632-73-3
- Product Name：2-Bromo-4-iodoaniline
- Molecular Formula：C6H5 Br I N
- Purity：98% GC
- Molecular Weight：297.921
Product Details
Top Quality 2-Bromo-4-iodoaniline 29632-73-3 Hot Sell In Stock
- Molecular Formula:C6H5 Br I N
- Molecular Weight:297.921
- Vapor Pressure:0.001mmHg at 25°C
- Melting Point:75-76 ºC
- Boiling Point:307.61°C at 760 mmHg
- Flash Point:139.838°C
- PSA：26.02000
- Density:2.292
- LogP:3.21710
2-Bromo-4-iodoaniline(Cas 29632-73-3) Usage
|
General Description |
2-Bromo-4-iodoaniline is a chemical compound consisting of an aniline ring with a bromine and iodine atom attached to it. It is a light yellow to brown solid, and is commonly used as an intermediate in organic synthesis, particularly in the pharmaceutical industry. 2-Bromo-4-iodoaniline is known to be toxic if ingested, inhaled, or absorbed through the skin, and can cause irritation to the respiratory system and skin. It has also been found to have mutagenic and carcinogenic properties, making it a hazardous material that requires careful handling and disposal. Additionally, 2-Bromo-4-iodoaniline may cause environmental harm if released into water or soil. Due to its potentially harmful effects, proper precautions and safety measures should be taken when working with this chemical. |
InChI:InChI=1/C6H5BrIN/c7-5-3-4(8)1-2-6(5)9/h1-3H,9H2
29632-73-3 Relevant articles
Bicyclic Phenyl–Ethynyl Architectures: Synthesis of a 1,4-Bis(phenylbuta-1,3-diyn-1-yl) Benzene Banister
Bannwart, Linda Maria,Müntener, Thomas,Rickhaus, Michel,Jundt, Lukas,H?ussinger, Daniel,Mayor, Marcel
, p. 6295 - 6307 (2021)
The novel diacetylene bridged terphenyli...
NOVEL RECYCLABLE IODINATING AGENT AND ITS APPLICATIONS
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Page/Page column 11; 15, (2016/11/07)
The present invention provides a novel r...
Regioselective iodination of aryl amines using 1,4-dibenzyl-1,4-diazoniabicyclo [2.2.2] octane dichloroiodate in solution and under solvent-free conditions
Alikarami, Mohammad,Nazarzadeh, Somayeh,Soleiman-Beigi, Mohammad
, p. 157 - 162 (2015/01/30)
1,4-Dibenzyl-1,4-diazoniabicyclo[2.2.2]o...
Recyclable ionic liquid iodinating reagent for solvent free, regioselective iodination of activated aromatic and heteroaromatic amines
Deshmukh, Amarsinh,Gore, Babasaheb,Thulasiram, Hirekodathakallu V.,Swamy, Vincent P.
, p. 88311 - 88315 (2015/11/09)
This article describes a simple, efficie...
29632-73-3 Process route
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615-36-1
2-bromoaniline
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29632-73-3
2-Bromo-4-iodoaniline
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873-38-1
4-chloro-2-bromoaniline
| Conditions | Yield |
|---|---|
|
With
1-butyl-3-methyl-pyridinium dichloroiodate;
for 1h;
|
86 %Chromat. 80 %Chromat. |
-
-
615-36-1
2-bromoaniline
-
-
29632-73-3
2-Bromo-4-iodoaniline
| Conditions | Yield |
|---|---|
|
With
N-iodo-succinimide;
In
dimethyl sulfoxide;
at 20 ℃;
for 18h;
|
98% |
|
With
1,4-dibenzyl-1,4-diazoniabicyclo[2.2.2]octane dichloroiodate;
In
neat (no solvent);
at 20 ℃;
for 0.333333h;
regioselective reaction;
|
88% |
|
With
N,N,N-trimethylbenzenemethanaminium dichloroiodate; calcium carbonate;
In
methanol; dichloromethane;
for 22h;
|
83% |
|
With
[K(18-crown-6)]ICl2; potassium carbonate;
In
acetonitrile;
at 50 ℃;
for 12h;
regioselective reaction;
|
72% |
|
With
sodium percarbonate; iodine; acetic acid;
In
ethyl acetate;
at 45 - 50 ℃;
for 3.5h;
|
67% |
|
With
iodine; periodic acid;
In
dichloromethane;
for 0.333333h;
Heating;
microwave irradiation;
|
14% |
|
With
sodium hydrogencarbonate; N,N,N-trimethylbenzenemethanaminium dichloroiodate;
In
methanol; dichloromethane;
at 20 ℃;
for 0.333333h;
|
1.34 g |
|
With
iodine; sodium hydrogencarbonate; aniline;
In
water; ethyl acetate;
|
2.53 g (91%) |
|
With
N-iodo-succinimide;
In
dimethyl sulfoxide;
at 20 ℃;
for 72h;
regioselective reaction;
|
29632-73-3 Upstream products
-
474966-95-5
N-(2-bromo-4-iodophenyl)acetamide
-
540-37-4
p-aminoiodobenzene
-
615-36-1
2-bromoaniline
-
103-84-4
Acetanilid
29632-73-3 Downstream products
-
873386-83-5
2-bromo-6-chloro-4-iodoaniline
-
860556-79-2
2-bromo-1,4-diiodobenzene
-
887603-49-8
2-bromo-1,4-bis-trimethylsilanylethynyl-benzene
-
887603-50-1
1-iodo-2,5-bis(trimethylsilylacetylene)benzene
Relevant Products
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-
4-Chloro-2-iodoanilineCAS：63069-48-7
-
cis-1,4-Dichloro-2-buteneCAS：1476-11-5