2969-81-5

  • Product Name:Ethyl 4-bromobutyrate
  • Molecular Formula:C6H11BrO2
  • Purity:98% GC
  • Molecular Weight:195.056
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Product Details

Ethyl 4-bromobutyrate GMP Manufacturer Global Trade 2969-81-5 with Fast Delivery

  • Molecular Formula:C6H11BrO2
  • Molecular Weight:195.056
  • Appearance/Colour:clear colorless to yellow liquid 
  • Vapor Pressure:0.362mmHg at 25°C 
  • Melting Point:98-100 °C 
  • Refractive Index:n20/D 1.456(lit.)  
  • Boiling Point:198.3 °C at 760 mmHg 
  • Flash Point:90.6 °C 
  • PSA:26.30000 
  • Density:1.352 g/cm3  
  • LogP:1.72460 

Ethyl 4-bromobutyrate(Cas 2969-81-5) Usage

Synthesis Reference(s)

The Journal of Organic Chemistry, 56, p. 2264, 1991 DOI: 10.1021/jo00006a061

InChI:InChI=1/C6H11BrO2/c1-2-9-6(8)4-3-5-7/h2-5H2,1H3

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2969-81-5 Process route

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ethyl 2,4-dibromobutyrate

Ethyl 4-bromobutyrate
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Ethyl 4-bromobutyrate

ethyl cyclopropylcarboxylate
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ethyl cyclopropylcarboxylate

butanoic acid ethyl ester
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butanoic acid ethyl ester

Conditions
Conditions Yield
In N,N-dimethyl-formamide; at 20 ℃; Product distribution; Mechanism; electrolysis; I*, napp; various conc. of the ester; in the presence and in the absence of 3,4-xylenol;
ethanol
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bromobutyric acid
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bromobutyric acid

Ethyl 4-bromobutyrate
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Ethyl 4-bromobutyrate

Conditions
Conditions Yield
bromobutyric acid; With oxalyl dichloride; N,N-dimethyl-formamide; In dichloromethane; at 20 ℃; for 5h;
ethanol; In dichloromethane; at 20 ℃; for 15h;
84%
With tetrachloromethane; 5-sulfosalicylic Acid; unter Entfernen des entstehenden Wassers;
With sulfuric acid;
With sulfuric acid;
With acetyl chloride; at 20 ℃; for 4h;

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