1227375-90-7

  • Product Name:1-[9-Ethyl-6-(2-methylbenzoyl)-9H-carbazol-3-yl]-3-cyclophentylpropanone-1-(O-acetyloxime)
  • Molecular Formula:
  • Purity:99%
  • Molecular Weight:494.634
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Product Details

Buy Quality 1-[9-Ethyl-6-(2-methylbenzoyl)-9H-carbazol-3-yl]-3-cyclophentylpropanone-1-(O-acetyloxime) 1227375-90-7 In Stock with Immediately Delivery

  • Molecular Formula:C32H34N2O3
  • Molecular Weight:494.634

1227375-90-7 Relevant articles

CARBAZOLE OXIME ESTER PHOTOINITIATOR

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Page/Page column 8, (2012/02/04)

A carbazole oxime ester photoinitiator a...

1227375-90-7 Process route

C<sub>30</sub>H<sub>32</sub>N<sub>2</sub>O<sub>2</sub>

C30H32N2O2

acetic anhydride
108-24-7

acetic anhydride

N-ethanoyloxy-1-[9-ethyl-6-(2-methylbenzoyl)-9H-carbazol-3-yl]-3-cyclopentaneylpropan-1-imine
1227375-90-7

N-ethanoyloxy-1-[9-ethyl-6-(2-methylbenzoyl)-9H-carbazol-3-yl]-3-cyclopentaneylpropan-1-imine

Conditions
Conditions Yield
C30H32N2O2; acetic anhydride; In dichloromethane; at 20 ℃; for 2.5h;
With sodium hydroxide; In dichloromethane; water;
N-ethylcarbazole
86-28-2

N-ethylcarbazole

N-ethanoyloxy-1-[9-ethyl-6-(2-methylbenzoyl)-9H-carbazol-3-yl]-3-cyclopentaneylpropan-1-imine
1227375-90-7

N-ethanoyloxy-1-[9-ethyl-6-(2-methylbenzoyl)-9H-carbazol-3-yl]-3-cyclopentaneylpropan-1-imine

Conditions
Conditions Yield
Multi-step reaction with 3 steps
1.1: aluminum (III) chloride / dichloromethane / 3.5 h / 0 - 10 °C / Inert atmosphere
1.2: 3.5 h / 10 - 15 °C / Inert atmosphere
2.1: hydroxylamine hydrochloride; sodium acetate / ethanol; water / 5 h / 10 °C / Reflux
3.1: dichloromethane / 2.5 h / 20 °C
With hydroxylamine hydrochloride; sodium acetate; aluminum (III) chloride; In ethanol; dichloromethane; water;

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